名稱：毛細(xì)管柱

固定液：聚乙二醇

規(guī)格：30m*0.32mm*0.25um

型號(hào)：HH-WAX

應(yīng)用：SN/T 4347-2015 進(jìn)出口化妝品中氯乙酰胺的測(cè)定 氣相色譜法

 2一氯乙酰胺是一種用在化妝品中的防腐劑,該品口服有毒,對(duì)呼吸系統(tǒng)和皮膚有刺激性,GB7916-1987中規(guī)定其為限 用物質(zhì),在化妝品中大允許濃度為0.3%.

浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司建立化妝品中2-氯乙酰胺的氣相色譜測(cè)定法。方法樣品用乙醇溶解,超聲波均質(zhì),離心,經(jīng)HH-Wax色譜柱分離,氫焰離子化檢測(cè)器檢測(cè)。結(jié)果2-氯乙酰胺濃度在0.0～10.0mg/ml范圍內(nèi)時(shí),該方法線性關(guān)系良好,檢出限小于0.01μg,相對(duì)標(biāo)準(zhǔn)偏差小于5.6%,回收率為90%～100%。結(jié)論該方法簡(jiǎn)便、快速、靈敏,適用于化妝品中2-氯乙酰胺的測(cè)定。

化妝品中2-氯乙酰胺的氣相色譜測(cè)定  測(cè)試譜圖：



Determination of 2-Chloroacetamide in Cosmetics by Gas Chromatography
Gas Chromatographic Determination of 2-Chloroacetamide in Cosmetics Details:

Name: capillary column

Fixative: polyethylene glycol

Specifications: 30m*0.32mm*0.25um

Model: HH-WAX

Application: SN/T 4347-2015 Determination of Chloroacetamide in import and Export Cosmetics-Gas Chromatography

 2-Chloroacetamide is a preservative used in cosmetics. This product is toxic to oral administration and is irritating to the respiratory system and skin. It is specified as a restricted substance in GB7916-1987, and the maximum allowable concentration in cosmetics is 0.3%. .

Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. established a gas chromatography method for the determination of 2-chloroacetamide in cosmetics. Methods The samples were dissolved in ethanol, homogenized by ultrasonic, centrifuged, separated by HH-Wax chromatographic column, and detected by hydrogen flame ionization detector. Results When the concentration of 2-chloroacetamide was in the range of 0.0～10.0mg/ml, the linearity of the method was good, the detection limit was less than 0.01μg, the relative standard deviation was less than 5.6%, and the recovery was 90%～100%. Conclusion The method is simple, rapid and sensitive, suitable for the determination of 2-chloroacetamide in cosmetics.

Determination of 2-Chloroacetamide in Cosmetics by Gas Chromatography Test Spectrum: