HH-CEC 一氯代碳酸乙烯酯的制備產物測定專用毛細管柱
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產品名稱：HH-CEC 一氯代碳酸乙烯酯的制備產物測定專用毛細管柱
產品型號：HH-CEC
產品廠商：浩瀚色譜（山東）應用技術開發(fā)有限公司
簡單介紹
HH-CEC 一氯代碳酸乙烯酯的制備產物測定專用毛細管柱的詳細介紹
一氯代碳酸乙烯酯的制備產物測定專用毛細管柱 詳細信息：
名稱：毛細管柱
規(guī)格：30m*0.32mm
型號：HH-CEC
一氯代碳酸乙烯酯的制備方法,包括:在塔式反應器內,沿塔高方向,每隔1米為一個填料層,安裝一個支架,每個支架底部安裝一個汞浸液燈,在每層填料的上方,分別安裝一個液體均布器和一個第二汞浸液燈;將碳酸乙烯酯預熱60℃,再加入引發(fā)劑和催化劑,加熱60℃,得含有引發(fā)劑和催化劑的碳酸乙烯酯液體;從塔底通入氮氣,置換塔內空氣,氮氣尾氣放空;氯氣干燥脫水后,加熱65℃,在塔底部和塔中部分別通入氯氣,從塔頂加入含有引發(fā)劑和催化。
浩瀚色譜（山東）應用技術開發(fā)有限公司，，，研發(fā)生產氯代碳酸乙烯酯制備過程測定的專用氣相色譜GC-，測定了一氯代碳酸乙烯酯和二氯代碳酸乙烯酯及殘存的原料碳酸乙烯酯的含量，柱效高，分離好，峰型對稱.此項技術為浩瀚色譜的。
其中原料碳酸乙烯酯（EC）:5.7062%;二氯碳酸乙烯酯（DCEC）:9.46%;氯代碳酸乙烯酯（CEC）:81.14%.
一氯代碳酸乙烯酯的制備產物測定專用毛細管柱 測試譜圖：
|
序號 |
保留時間 |
組分名稱 |
濃度 |
峰面積 |
峰高 |
結果判定 |
|
1 |
0.979 |
|
0.0213 |
1290 |
293 |
|
|
2 |
1.148 |
|
0.0859 |
5194 |
3981 |
|
|
3 |
1.619 |
|
0.0411 |
2485 |
413 |
|
|
4 |
1.739 |
|
0.1764 |
10669 |
1124 |
|
|
5 |
2.099 |
|
0.0235 |
1420 |
152 |
|
|
6 |
2.549 |
|
0.0486 |
2942 |
189 |
|
|
7 |
3.259 |
|
0.0265 |
1601 |
184 |
|
|
8 |
5.154 |
|
0.0215 |
1298 |
378 |
|
|
9 |
6.224 |
|
0.0272 |
1646 |
552 |
|
|
10 |
7.355 |
|
0.0229 |
1388 |
237 |
|
|
11 |
8.468 |
|
0.4619 |
27945 |
9114 |
|
|
12 |
10.482 |
|
0.0287 |
1735 |
447 |
|
|
13 |
11.267 |
EC |
5.7062 |
345214 |
104380 |
碳酸乙烯酯 |
|
14 |
11.972 |
|
0.0302 |
1824 |
318 |
|
|
15 |
12.584 |
|
0.2179 |
13181 |
3644 |
|
|
16 |
13.119 |
|
0.0911 |
5514 |
1547 |
|
|
17 |
13.470 |
|
0.0463 |
2801 |
746 |
|
|
18 |
13.839 |
|
0.3849 |
23287 |
6486 |
|
|
19 |
14.117 |
|
0.3071 |
18582 |
2902 |
|
|
20 |
14.364 |
|
0.0282 |
1708 |
384 |
|
|
21 |
15.038 |
DCEC |
9.4644 |
572580 |
64020 |
二氯碳酸乙烯酯 |
|
22 |
15.226 |
|
0.1868 |
11300 |
2977 |
|
|
23 |
15.608 |
|
0.0392 |
2372 |
532 |
|
|
24 |
16.297 |
CEC |
81.1464 |
4909204 |
399048 |
氯代碳酸乙烯酯 |
|
25 |
16.813 |
|
0.0230 |
1392 |
296 |
|
|
26 |
17.067 |
|
0.0382 |
2312 |
678 |
|
|
27 |
17.373 |
|
0.2833 |
17142 |
3597 |
|
|
28 |
17.702 |
|
0.0406 |
2458 |
746 |
|
|
29 |
18.118 |
|
0.0692 |
4187 |
1158 |
|
|
30 |
18.573 |
|
0.1265 |
7654 |
1376 |
|
|
31 |
20.102 |
|
0.0313 |
1896 |
446 |
|
|
32 |
20.438 |
|
0.0197 |
1190 |
342 |
|
|
33 |
21.371 |
|
0.0052 |
318 |
160 |
|
|
34 |
21.825 |
|
0.1062 |
6426 |
690 |
|
|
35 |
22.209 |
|
0.0109 |
659 |
319 |
|
|
36 |
22.360 |
|
0.0202 |
1223 |
403 |
|
|
37 |
22.805 |
|
0.0831 |
5029 |
239 |
|
|
38 |
23.450 |
|
0.1838 |
11120 |
911 |
|
|
39 |
23.696 |
|
0.0346 |
2091 |
308 |
|
|
40 |
24.329 |
|
0.0436 |
2637 |
252 |
|
|
41 |
24.570 |
|
0.0167 |
1011 |
277 |
|
|
42 |
24.730 |
|
0.0101 |
614 |
227 |
|
|
43 |
24.917 |
|
0.0357 |
2161 |
236 |
|
|
44 |
25.637 |
|
0.1837 |
11112 |
377 |
|
Special capillary column for the determination of preparation products of mo
Special capillary column for the determination of preparation products of mo
Name: capillary column
Specifications: 30m*0.32mm
Model: HH-CEC
The preparation method of mo
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd., keeping pace with the times and guided by the scientific development concept, has developed and produced a special gas chromatography GC- for the determination of the preparation process of chloroethylene carbonate. The co
Among them, the raw material ethylene carbo
Special capillary column for the determination of the preparation product of mo
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